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ELECTRONIC DEVICE FAILURE ANALYSIS | VOLUME 19 NO. 2

interface. Often, APT laser power, evaporation rate, or

other parameters arealtered tohelpwithfieldevaporation

through delicate or problematic interfaces to avoid pre-

mature tip rupture. However, it is important tounderstand

the effects of altering such parameters on the integrity of

the collecteddata. For example, increasing the laser power

to assist field evaporation of a thin oxide layer may force

the overall evaporation field in the surrounding silicon

to stray from optimal. Likewise, decreasing the evapo-

ration rate when moving through a region of insulating

materials (e.g., gate oxide or spacer) to keep the tip from

fracturingmay significantly increase noise levels, making

low dopant profiles in nearby SiGe source/drain regions

more difficult to measure. These various trade-offs must

be considered, and remaining artifacts, noise, and so

on must be understood and properly interpreted if they

cannot yet be eliminated.

CONCLUSION

Atom probe tomography has a unique capability to

analyze even the most complex structures. Its combina-

tion of structural and chemical information for buried

nanostructures makes it a one-of-a-kind resource in a

number of fields and particularly for semiconductor

devices. Atom probe tomography helps provide a clearer

understanding of the shape and elemental composition

of complex device structures and light dopant profile

throughout these structures. Although many challenges

still remain for samplepreparation, improvedunderstand-

ing of APT data collection, and, most significantly, elimi-

nation of artifacts from the reconstructed 3-D data, APT

remains a powerful tool for failure analysis and research

and development of the next generation of advanced

semiconductor devices.

REFERENCES

1. A.J. Martin, W. Weng, Z. Zhu, R. Loesing, J. Shaffer, and A. Katnani:

“Cross-Sectional Atom Probe Tomography Sample Preparation for

Improved Analysis of Fins on SOI,”

Ultramicroscopy,

2016,

161

, pp.

105-09.

2. A.J. Martin, A.H. Hunter, T.W. Saucer, V. Sih, E.A. Marquis, and J.

Millunchick: “Atom Probe Tomography Analysis of Different Modes

of Sb Intermixing inGaSbQuantumDots andWells,”

Appl. Phys. Lett.,

2013,

103

, p. 122102.

3. A.K. Kambham, J. Mody, M. Gilbert, S. Koelling, and W. Vandervorst:

“Atom-Probe for FinFET Dopant Characterization,”

Ultramicroscopy,

2011, pp. 535-39.

4. D.R. Diercks, J. Tong, H. Zhu, R. Kee, G. Baure, J.C. Nino, R. O’Hayre,

Fig. 7

STEM images of a different APT tip shaped from the same sample. (a) Plan-view perspective of the tip with various

features labeled. (b) Rotated view of the SiGe, highlighting the wavy shape of the outer surface of the tip. Scale bars

not shown for proprietary reasons

(continued on page 30)