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A D V A N C E D M A T E R I A L S & P R O C E S S E S | J U N E 2 0 1 6

1 0

TESTING | CHARACTERIZATION

approximately 20 cm, and a resolution

of 20 µm. Eventually the researchers

will test a second lens capable of 1-µm

resolution, allowing for an estimated

10-fold increase in spatial resolution

over what is currently possible.

Neutron imaging allows scientists

to see aspects of objects not visible

with light, such as the inner workings

of batteries and metals under strain.

For example, the newmicroscope could

look inside the catalyst layer of a hydro-

gen fuel cell, which is on the order of

1-10 µm, and give scientists a first look

at the water transport processes taking

place there

. nist.gov.

ELECTRODE RECONFIGURATION,

ENHANCED INFORMATION

Researchers at Argonne National

Laboratory, Lemont, Ill., demonstrated

that a new configuration of reference

electrodes—devices used to measure

voltage in individual electrodes within

a battery cell—can improve the quan-

tity and quality of information obtained

from lithium-ion battery cells during

cycling. Previously, Argonne research-

ers used only one reference electrode,

based on a lithium-tin (Li-Sn) alloy.

However, the team discovered that

sandwiching a Li-Sn reference electrode

between the positive and negative elec-

trodes, with a pure lithium reference

electrode positioned next to the stack,

provided insight into electrode state-of-

charge shifts, activematerial use, active

material loss, and impedance changes.

NEUTRON MICROSCOPE

COMING INTO FOCUS

In the quest to produce the world’s

first workhorse neutron microscope,

scientists from NIST’s Physical Mea-

surement Laboratory (PML), in collabo-

ration with NASA and MIT researchers,

are approaching a milestone—a new

prototype for a neutron lens. The lens

is based on a

Wolter optic,

a series of

nested conical mirrors made of thin lay-

ers of highly polished nickel. The design

allows neutrons, which pass through

mirrors unless they strike them at a low

angle of incidence, to be concentrated

onto a specimen. The lens in develop-

ment will consist of about 10 nested

mirror shells, with amaximumdiameter

of approximately 5 cm, a total length of

A THz-frequency materials charac-

terization system from

Lake Shore

Cryotronics,

Westerville, Ohio, was

installed in the lab of professor Dan

Mittleman at

Brown University,

Providence, R.I. Mittleman’s team

is exploring how frequencies within

the terahertz band of the electro-

magnetic spectrum can advance

spectroscopic studies of materials,

and the 8500 Series system will

be used primarily to study

THz-frequency magneto-optical

responses of semimetals, iron-base

superconductors, and other novel

materials.

lakeshore.com

.

BRIEFS

Thermal management technology developer

Gentherm,

Northville,

Mich., acquired

Cincinnati Sub-Zero Products

(CSZ). CSZ manufactures

custom environmental test chambers used for product testing in

industrial manufacturing. The company had revenues of approximately

$63 million in 2015 and will be operated as a subsidiary of Gentherm,

with its headquarters in Cincinnati and operations in Ohio and Michigan.

gentherm.com

.

DanHussey in the shielded cavewhere the neutronmicroscopewill be housedat NIST.

Unique CW-THz spectroscopy systemwill aid

the Mittleman Lab in materials research.